MIKIO KUZUYA, PROFESSOR
B.Eng. Nagoya University, 1975
Ph.D. Nagoya University, 1983
Dr. Kuzuya's research
is concerned with the analytical applications of lasers. A high-power laser
beam, such as a Q-switched Nd:YAG laser focused onto the surface of the
sample ablates and atmoizes a small amount of sample, and induces a luminous
plasma which consists of neutral and charged particles (atoms, molecules, ions,
and electrons). The laser-induced plasmas are used as the sources for optical
emission spectrometry (LMA-OES) and mass spectrometry (LMA-MS).
Most work in his laboratory concentrates on the development/improvement of Laser
Microprobe Analysis(LMA) system,
such as LMA-OES and LMA-MS. LMA is one of several methods for
direct chemical analysis of solids and has unique capabilities of analyzing
microareas of any type of material, including electically nonconductive materials,
without sample preparation.
Brief contents:
LMA-OES: Analysis
method for determinations of the concentrations of chemical elements of samples
by spectrally resolving the light from the laser-induced plasma. In order to
improve the analytical performance, the effects of the ambient atmosphere(kinds,
pressure) and the laser(energy, focusing) on the emission characteristics of
the laser-induced plasma are being studied by using time- and space-resolved
spectroscopy.
LMA-MS: Two types
of laser mass spectrometric methods are being studied. (1)Laser Ablation Mass
Spectrometry(LAMS) is a combination of laser ablation of sample materials,
electron inoization of atoms and molecules, and mass spectrometric seperation
technique. (2)Laser Ionization Mass Spectrometry(LIMS)
is based on the ionization of atoms and molecules in a microplasma produced
by the irradiation of a high-power laser. Gas-phase ions are analyzed by mass
spectroscopy.
Recently, we have initated
studies of Laser Microprobe Gas Chromatography(LM-GC) which uses a laser
as a fragmentation source for gas chromatography. This method is applicable
to direct analysis of nonvolatile samples.
Peripheral instruments
and system for LMA described below are being designed and constructed
in our laboratory.
1. Pulse generator for controlling the timing of the LMA system
2. Laser energy monitor
3. Stepping motor driver
4. Plasma monitor system with a CCD video camera and a digital image processing computer
5. Software for data processing
6. Data acquisition system using A/D converter
7. Other electronic circuits
(Design of the pattern of electronic circuit is carried out by using CAD system)
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